Polysiloxane deactivated fused silica capillaries containing immobilized stationary phases


Journal Article

This article describes a method of preparing immobilized stationary phases which has arisen from the authors' work on polysiloxane deactivation of fused silica capillaries. Although acid treatment is often omitted with fused silica capillaries, there are good reasons for hydrothermal treatment of this column material. Use of Grob's peroxide method gave immobilized 0.25 μm films of SE‐54; lowering of the immobilization temperature permitted immobilization of 0.1 μm films of the same phase. Copyright © 1982 Dr. Alfred Hüthig Verlag GmbH

Full Text

Duke Authors

Cited Authors

  • Moseley, MA; Pellizzari, ED

Published Date

  • January 1, 1982

Published In

Volume / Issue

  • 5 / 9

Start / End Page

  • 472 - 475

Electronic International Standard Serial Number (EISSN)

  • 1521-4168

International Standard Serial Number (ISSN)

  • 0935-6304

Digital Object Identifier (DOI)

  • 10.1002/jhrc.1240050904

Citation Source

  • Scopus