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Polysiloxane deactivated fused silica capillaries containing immobilized stationary phases

Publication ,  Journal Article
Moseley, MA; Pellizzari, ED
Published in: Journal of High Resolution Chromatography
January 1, 1982

This article describes a method of preparing immobilized stationary phases which has arisen from the authors' work on polysiloxane deactivation of fused silica capillaries. Although acid treatment is often omitted with fused silica capillaries, there are good reasons for hydrothermal treatment of this column material. Use of Grob's peroxide method gave immobilized 0.25 μm films of SE‐54; lowering of the immobilization temperature permitted immobilization of 0.1 μm films of the same phase. Copyright © 1982 Dr. Alfred Hüthig Verlag GmbH

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Published In

Journal of High Resolution Chromatography

DOI

EISSN

1521-4168

ISSN

0935-6304

Publication Date

January 1, 1982

Volume

5

Issue

9

Start / End Page

472 / 475

Related Subject Headings

  • Analytical Chemistry
  • 0601 Biochemistry and Cell Biology
  • 0399 Other Chemical Sciences
  • 0301 Analytical Chemistry
 

Citation

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Moseley, M. A., & Pellizzari, E. D. (1982). Polysiloxane deactivated fused silica capillaries containing immobilized stationary phases. Journal of High Resolution Chromatography, 5(9), 472–475. https://doi.org/10.1002/jhrc.1240050904
Moseley, M. A., and E. D. Pellizzari. “Polysiloxane deactivated fused silica capillaries containing immobilized stationary phases.” Journal of High Resolution Chromatography 5, no. 9 (January 1, 1982): 472–75. https://doi.org/10.1002/jhrc.1240050904.
Moseley MA, Pellizzari ED. Polysiloxane deactivated fused silica capillaries containing immobilized stationary phases. Journal of High Resolution Chromatography. 1982 Jan 1;5(9):472–5.
Moseley, M. A., and E. D. Pellizzari. “Polysiloxane deactivated fused silica capillaries containing immobilized stationary phases.” Journal of High Resolution Chromatography, vol. 5, no. 9, Jan. 1982, pp. 472–75. Scopus, doi:10.1002/jhrc.1240050904.
Moseley MA, Pellizzari ED. Polysiloxane deactivated fused silica capillaries containing immobilized stationary phases. Journal of High Resolution Chromatography. 1982 Jan 1;5(9):472–475.

Published In

Journal of High Resolution Chromatography

DOI

EISSN

1521-4168

ISSN

0935-6304

Publication Date

January 1, 1982

Volume

5

Issue

9

Start / End Page

472 / 475

Related Subject Headings

  • Analytical Chemistry
  • 0601 Biochemistry and Cell Biology
  • 0399 Other Chemical Sciences
  • 0301 Analytical Chemistry