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Light scattering study of polydimethyl siloxane in liquid and supercritical carbon dioxide

Publication ,  Journal Article
Andr, P; Folk, SL; Adam, M; Rubinstein, M; DeSimone, JM
Published in: Journal of Physical Chemistry A
2004

In this paper, we report the results of static and dynamic light scattering investigations of polydimethyl siloxane (PDMS) solutions in both liquid and supercritical carbon dioxide (CO2). This study was performed below the theta point and provides quantitative information on the CO2 solvent quality over a large range of temperature (25-54 degreesC) and density (0.97-1.01 g/mL). The solvent quality of the CO2 can be adjusted by independently varying temperature or density, as demonstrated by the dependence of the second virial coefficient on these two parameters. The theta temperature was observed to be a strong function of CO2 density and may be a weak function of the PDMS molecular weight. The strength of the excluded volume interactions in the PDMS-CO2 solution was determined to be weaker than predicted, and no universal behavior was observed.

Duke Scholars

Published In

Journal of Physical Chemistry A

DOI

ISSN

1089-5639

Publication Date

2004

Related Subject Headings

  • 5102 Atomic, molecular and optical physics
  • 3407 Theoretical and computational chemistry
  • 3406 Physical chemistry
  • 0307 Theoretical and Computational Chemistry
  • 0306 Physical Chemistry (incl. Structural)
  • 0202 Atomic, Molecular, Nuclear, Particle and Plasma Physics
 

Citation

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Andr, P., Folk, S. L., Adam, M., Rubinstein, M., & DeSimone, J. M. (2004). Light scattering study of polydimethyl siloxane in liquid and supercritical carbon dioxide. Journal of Physical Chemistry A. https://doi.org/10.1021/jp0481308
Andr, Pascal, Sarah L. Folk, Mireille Adam, Michael Rubinstein, and Joseph M. DeSimone. “Light scattering study of polydimethyl siloxane in liquid and supercritical carbon dioxide.” Journal of Physical Chemistry A, 2004. https://doi.org/10.1021/jp0481308.
Andr P, Folk SL, Adam M, Rubinstein M, DeSimone JM. Light scattering study of polydimethyl siloxane in liquid and supercritical carbon dioxide. Journal of Physical Chemistry A. 2004;
Andr, Pascal, et al. “Light scattering study of polydimethyl siloxane in liquid and supercritical carbon dioxide.” Journal of Physical Chemistry A, 2004. Manual, doi:10.1021/jp0481308.
Andr P, Folk SL, Adam M, Rubinstein M, DeSimone JM. Light scattering study of polydimethyl siloxane in liquid and supercritical carbon dioxide. Journal of Physical Chemistry A. 2004;
Journal cover image

Published In

Journal of Physical Chemistry A

DOI

ISSN

1089-5639

Publication Date

2004

Related Subject Headings

  • 5102 Atomic, molecular and optical physics
  • 3407 Theoretical and computational chemistry
  • 3406 Physical chemistry
  • 0307 Theoretical and Computational Chemistry
  • 0306 Physical Chemistry (incl. Structural)
  • 0202 Atomic, Molecular, Nuclear, Particle and Plasma Physics