Synthesis of Δ11-9α-fluoro-steroids: X-ray crystal and molecular structure of 17α,21-dipropionyloxy-9α-fluoro-16β- methylpregna-1,4,11-triene-3,20-dione
Publication
, Journal Article
Green, MJ; Shue, HJ; Tanabe, M; Yasuda, DM; McPhail, AT; Onan, KD
Published in: Journal of the Chemical Society, Chemical Communications
December 1, 1977
Reaction of 9α-fluoro-corticosteroids with NN-dialkylaminosulphur trifluorides gives Δ11-9α-fluoro-steroids (2a,b); a single-crystal X-ray analysis of (2a) is reported.
Duke Scholars
Published In
Journal of the Chemical Society, Chemical Communications
DOI
ISSN
0022-4936
Publication Date
December 1, 1977
Issue
17
Start / End Page
611 / 612
Citation
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Green, M. J., Shue, H. J., Tanabe, M., Yasuda, D. M., McPhail, A. T., & Onan, K. D. (1977). Synthesis of Δ11-9α-fluoro-steroids: X-ray crystal and molecular structure of 17α,21-dipropionyloxy-9α-fluoro-16β- methylpregna-1,4,11-triene-3,20-dione. Journal of the Chemical Society, Chemical Communications, (17), 611–612. https://doi.org/10.1039/C39770000611
Green, M. J., H. J. Shue, M. Tanabe, D. M. Yasuda, A. T. McPhail, and K. D. Onan. “Synthesis of Δ11-9α-fluoro-steroids: X-ray crystal and molecular structure of 17α,21-dipropionyloxy-9α-fluoro-16β- methylpregna-1,4,11-triene-3,20-dione.” Journal of the Chemical Society, Chemical Communications, no. 17 (December 1, 1977): 611–12. https://doi.org/10.1039/C39770000611.
Green MJ, Shue HJ, Tanabe M, Yasuda DM, McPhail AT, Onan KD. Synthesis of Δ11-9α-fluoro-steroids: X-ray crystal and molecular structure of 17α,21-dipropionyloxy-9α-fluoro-16β- methylpregna-1,4,11-triene-3,20-dione. Journal of the Chemical Society, Chemical Communications. 1977 Dec 1;(17):611–2.
Green, M. J., et al. “Synthesis of Δ11-9α-fluoro-steroids: X-ray crystal and molecular structure of 17α,21-dipropionyloxy-9α-fluoro-16β- methylpregna-1,4,11-triene-3,20-dione.” Journal of the Chemical Society, Chemical Communications, no. 17, Dec. 1977, pp. 611–12. Scopus, doi:10.1039/C39770000611.
Green MJ, Shue HJ, Tanabe M, Yasuda DM, McPhail AT, Onan KD. Synthesis of Δ11-9α-fluoro-steroids: X-ray crystal and molecular structure of 17α,21-dipropionyloxy-9α-fluoro-16β- methylpregna-1,4,11-triene-3,20-dione. Journal of the Chemical Society, Chemical Communications. 1977 Dec 1;(17):611–612.
Published In
Journal of the Chemical Society, Chemical Communications
DOI
ISSN
0022-4936
Publication Date
December 1, 1977
Issue
17
Start / End Page
611 / 612