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Low-temperature 13C magnetic resonance. 8. Chemical shielding anisotropy of olefinic carbons

Publication ,  Journal Article
Orendt, AM; Facelli, JC; Beeler, AJ; Reuter, K; Horton, WJ; Cutts, P; Grant, DM; Michl, J
Published in: Journal of the American Chemical Society
January 1, 1988

The principal values of the 13C NMR shielding tensor were measured at cryogenic temperatures for a series of olefinic carbons, including methyl-substituted ethylenes, 1-methyl- and 1,2-dimethylcycloalkenes, methylenecycloalkanes, and bicyclo[n.m.0]alkenes. Information on the orientation of the principal axes was obtained from ab initio calculations of the chemical shielding tensors using the IGLO (individual gauge for localized orbitals) method. The results for several compounds with unusual principal values of the shielding tensor were analyzed in terms of the bond contributions in the principal axis system. © 1988, American Chemical Society. All rights reserved.

Duke Scholars

Published In

Journal of the American Chemical Society

DOI

EISSN

1520-5126

ISSN

0002-7863

Publication Date

January 1, 1988

Volume

110

Issue

11

Start / End Page

3386 / 3392

Related Subject Headings

  • General Chemistry
  • 40 Engineering
  • 34 Chemical sciences
  • 03 Chemical Sciences
 

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Orendt, A. M., Facelli, J. C., Beeler, A. J., Reuter, K., Horton, W. J., Cutts, P., … Michl, J. (1988). Low-temperature 13C magnetic resonance. 8. Chemical shielding anisotropy of olefinic carbons. Journal of the American Chemical Society, 110(11), 3386–3392. https://doi.org/10.1021/ja00219a007
Orendt, A. M., J. C. Facelli, A. J. Beeler, K. Reuter, W. J. Horton, P. Cutts, D. M. Grant, and J. Michl. “Low-temperature 13C magnetic resonance. 8. Chemical shielding anisotropy of olefinic carbons.” Journal of the American Chemical Society 110, no. 11 (January 1, 1988): 3386–92. https://doi.org/10.1021/ja00219a007.
Orendt AM, Facelli JC, Beeler AJ, Reuter K, Horton WJ, Cutts P, et al. Low-temperature 13C magnetic resonance. 8. Chemical shielding anisotropy of olefinic carbons. Journal of the American Chemical Society. 1988 Jan 1;110(11):3386–92.
Orendt, A. M., et al. “Low-temperature 13C magnetic resonance. 8. Chemical shielding anisotropy of olefinic carbons.” Journal of the American Chemical Society, vol. 110, no. 11, Jan. 1988, pp. 3386–92. Scopus, doi:10.1021/ja00219a007.
Orendt AM, Facelli JC, Beeler AJ, Reuter K, Horton WJ, Cutts P, Grant DM, Michl J. Low-temperature 13C magnetic resonance. 8. Chemical shielding anisotropy of olefinic carbons. Journal of the American Chemical Society. 1988 Jan 1;110(11):3386–3392.
Journal cover image

Published In

Journal of the American Chemical Society

DOI

EISSN

1520-5126

ISSN

0002-7863

Publication Date

January 1, 1988

Volume

110

Issue

11

Start / End Page

3386 / 3392

Related Subject Headings

  • General Chemistry
  • 40 Engineering
  • 34 Chemical sciences
  • 03 Chemical Sciences