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Rapid (<3 min) microwave synthesis of block copolymer templated ordered mesoporous metal oxide and carbonate films using nitrate-citric acid systems.

Publication ,  Journal Article
Zhang, Y; Bhaway, SM; Wang, Y; Cavicchi, KA; Becker, ML; Vogt, BD
Published in: Chemical communications (Cambridge, England)
March 2015

Rapid chemical transformation from micelle templated precursors (metal nitrate and citric acid) to ordered mesoporous metal carbonates and oxides is demonstrated using microwave heating for cobalt, copper, manganese and zinc. Without aging requirements, <3 min of microwave processing yields highly ordered mesoporous films.

Duke Scholars

Published In

Chemical communications (Cambridge, England)

DOI

EISSN

1364-548X

ISSN

1359-7345

Publication Date

March 2015

Volume

51

Issue

24

Start / End Page

4997 / 5000

Related Subject Headings

  • Zinc
  • Surface Properties
  • Porosity
  • Polymers
  • Particle Size
  • Oxides
  • Organic Chemistry
  • Nitrates
  • Microwaves
  • Manganese
 

Citation

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ICMJE
MLA
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Zhang, Y., Bhaway, S. M., Wang, Y., Cavicchi, K. A., Becker, M. L., & Vogt, B. D. (2015). Rapid (<3 min) microwave synthesis of block copolymer templated ordered mesoporous metal oxide and carbonate films using nitrate-citric acid systems. Chemical Communications (Cambridge, England), 51(24), 4997–5000. https://doi.org/10.1039/c4cc09808k
Zhang, Yuanzhong, Sarang M. Bhaway, Yi Wang, Kevin A. Cavicchi, Matthew L. Becker, and Bryan D. Vogt. “Rapid (<3 min) microwave synthesis of block copolymer templated ordered mesoporous metal oxide and carbonate films using nitrate-citric acid systems.Chemical Communications (Cambridge, England) 51, no. 24 (March 2015): 4997–5000. https://doi.org/10.1039/c4cc09808k.
Zhang Y, Bhaway SM, Wang Y, Cavicchi KA, Becker ML, Vogt BD. Rapid (<3 min) microwave synthesis of block copolymer templated ordered mesoporous metal oxide and carbonate films using nitrate-citric acid systems. Chemical communications (Cambridge, England). 2015 Mar;51(24):4997–5000.
Zhang, Yuanzhong, et al. “Rapid (<3 min) microwave synthesis of block copolymer templated ordered mesoporous metal oxide and carbonate films using nitrate-citric acid systems.Chemical Communications (Cambridge, England), vol. 51, no. 24, Mar. 2015, pp. 4997–5000. Epmc, doi:10.1039/c4cc09808k.
Zhang Y, Bhaway SM, Wang Y, Cavicchi KA, Becker ML, Vogt BD. Rapid (<3 min) microwave synthesis of block copolymer templated ordered mesoporous metal oxide and carbonate films using nitrate-citric acid systems. Chemical communications (Cambridge, England). 2015 Mar;51(24):4997–5000.
Journal cover image

Published In

Chemical communications (Cambridge, England)

DOI

EISSN

1364-548X

ISSN

1359-7345

Publication Date

March 2015

Volume

51

Issue

24

Start / End Page

4997 / 5000

Related Subject Headings

  • Zinc
  • Surface Properties
  • Porosity
  • Polymers
  • Particle Size
  • Oxides
  • Organic Chemistry
  • Nitrates
  • Microwaves
  • Manganese