Scholars@Duke publication: Preparation and X-ray crystal structure of a novel tetranuclear copper(I) ethylenethiourea cluster complex, μ4-ethylenethiourea-cyclo- tetrakis-μ-(ethylenethiourea)tetrakis[ethylenethioureacopper(I)] nitrate hexahydrate

Preparation and X-ray crystal structure of a novel tetranuclear copper(I) ethylenethiourea cluster complex, μ4-ethylenethiourea-cyclo- tetrakis-μ-(ethylenethiourea)tetrakis[ethylenethioureacopper(I)] nitrate hexahydrate

Journal articles - Journal Article

Crumbliss, AL; Gestaut, LJ; Rickard, RC; McPhail, AT

Published in: Journal of the Chemical Society Chemical Communications

January 1, 1974

Published version (DOI)

The structure, geometry, and bonding in [Cu4(C3H 6N2S)9(NO3)4],6H 2O have been established by X-ray analysis which reveals discrete Cu4(C3H6N2S)9 ⁴⁺ cations containing an alternating Cu-S eight-membered ring with a unique ethylenethiourea ligand in an axial position bridging four copper atoms.

Duke Scholars

Author Alvin L. Crumbliss Chemistry

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Published In

Journal of the Chemical Society Chemical Communications

DOI

10.1039/C39740000545

ISSN

0022-4936

Publication Date

January 1, 1974

Issue

14

Start / End Page

545 / 546

Citation

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Crumbliss, A. L., Gestaut, L. J., Rickard, R. C., & McPhail, A. T. (1974). Preparation and X-ray crystal structure of a novel tetranuclear copper(I) ethylenethiourea cluster complex, μ4-ethylenethiourea-cyclo- tetrakis-μ-(ethylenethiourea)tetrakis[ethylenethioureacopper(I)] nitrate hexahydrate. Journal of the Chemical Society Chemical Communications, (14), 545–546. https://doi.org/10.1039/C39740000545

Crumbliss, A. L., L. J. Gestaut, R. C. Rickard, and A. T. McPhail. “Preparation and X-ray crystal structure of a novel tetranuclear copper(I) ethylenethiourea cluster complex, μ4-ethylenethiourea-cyclo- tetrakis-μ-(ethylenethiourea)tetrakis[ethylenethioureacopper(I)] nitrate hexahydrate.” Journal of the Chemical Society Chemical Communications, no. 14 (January 1, 1974): 545–46. https://doi.org/10.1039/C39740000545.

Crumbliss AL, Gestaut LJ, Rickard RC, McPhail AT. Preparation and X-ray crystal structure of a novel tetranuclear copper(I) ethylenethiourea cluster complex, μ4-ethylenethiourea-cyclo- tetrakis-μ-(ethylenethiourea)tetrakis[ethylenethioureacopper(I)] nitrate hexahydrate. Journal of the Chemical Society Chemical Communications. 1974 Jan 1;(14):545–6.

Crumbliss, A. L., et al. “Preparation and X-ray crystal structure of a novel tetranuclear copper(I) ethylenethiourea cluster complex, μ4-ethylenethiourea-cyclo- tetrakis-μ-(ethylenethiourea)tetrakis[ethylenethioureacopper(I)] nitrate hexahydrate.” Journal of the Chemical Society Chemical Communications, no. 14, Jan. 1974, pp. 545–46. Scopus, doi:10.1039/C39740000545.

Crumbliss AL, Gestaut LJ, Rickard RC, McPhail AT. Preparation and X-ray crystal structure of a novel tetranuclear copper(I) ethylenethiourea cluster complex, μ4-ethylenethiourea-cyclo- tetrakis-μ-(ethylenethiourea)tetrakis[ethylenethioureacopper(I)] nitrate hexahydrate. Journal of the Chemical Society Chemical Communications. 1974 Jan 1;(14):545–546.

Published In

Journal of the Chemical Society Chemical Communications

DOI

10.1039/C39740000545

ISSN

0022-4936

Publication Date

January 1, 1974

Issue

14

Start / End Page

545 / 546