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A refocused and optimized HNCA: increased sensitivity and resolution in large macromolecules.

Publication ,  Journal Article
Farmer, BT; Venters, RA; Spicer, LD; Wittekind, MG; Müller, L
Published in: J Biomol NMR
March 1992

A 3D optimized, refocused HNCA experiment is described. It is demonstrated to yield a dramatic increase in sensitivity when applied to [13C, 15N]-labeled human carbonic anhydrase II, a 29-kDa protein. The reasons for the gain in sensitivity are discussed, and 3 distinct areas for further development are indicated.

Duke Scholars

Published In

J Biomol NMR

DOI

ISSN

0925-2738

Publication Date

March 1992

Volume

2

Issue

2

Start / End Page

195 / 202

Location

Netherlands

Related Subject Headings

  • Protein Conformation
  • Nitrogen Isotopes
  • Mathematics
  • Magnetic Resonance Spectroscopy
  • Isoenzymes
  • Humans
  • Carbonic Anhydrases
  • Carbon Isotopes
  • Biophysics
  • 51 Physical sciences
 

Citation

APA
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ICMJE
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Farmer, B. T., Venters, R. A., Spicer, L. D., Wittekind, M. G., & Müller, L. (1992). A refocused and optimized HNCA: increased sensitivity and resolution in large macromolecules. J Biomol NMR, 2(2), 195–202. https://doi.org/10.1007/BF01875530
Farmer, B. T., R. A. Venters, L. D. Spicer, M. G. Wittekind, and L. Müller. “A refocused and optimized HNCA: increased sensitivity and resolution in large macromolecules.J Biomol NMR 2, no. 2 (March 1992): 195–202. https://doi.org/10.1007/BF01875530.
Farmer BT, Venters RA, Spicer LD, Wittekind MG, Müller L. A refocused and optimized HNCA: increased sensitivity and resolution in large macromolecules. J Biomol NMR. 1992 Mar;2(2):195–202.
Farmer, B. T., et al. “A refocused and optimized HNCA: increased sensitivity and resolution in large macromolecules.J Biomol NMR, vol. 2, no. 2, Mar. 1992, pp. 195–202. Pubmed, doi:10.1007/BF01875530.
Farmer BT, Venters RA, Spicer LD, Wittekind MG, Müller L. A refocused and optimized HNCA: increased sensitivity and resolution in large macromolecules. J Biomol NMR. 1992 Mar;2(2):195–202.
Journal cover image

Published In

J Biomol NMR

DOI

ISSN

0925-2738

Publication Date

March 1992

Volume

2

Issue

2

Start / End Page

195 / 202

Location

Netherlands

Related Subject Headings

  • Protein Conformation
  • Nitrogen Isotopes
  • Mathematics
  • Magnetic Resonance Spectroscopy
  • Isoenzymes
  • Humans
  • Carbonic Anhydrases
  • Carbon Isotopes
  • Biophysics
  • 51 Physical sciences